N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

Base Information

Chemical Name:N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide
CAS No.:736148-55-3
Molecular Formula:C₄₈H₂₆N₆O₈
Molecular Weight:814.77
Hs Code.:

Synonyms:N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

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Chemical Property of N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

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Technology Process of N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

There total 3 articles about N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 106-50-3
1,4-phenylenediamine

: 1,7-bis(p-nitrophenyl)-3,4:9,10-perylenetetracarboxydianhydride

: 736148-55-3
N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

Guidance literature:: With pyridine; 1H-imidazole; for 6h; Heating;
DOI:10.1021/ja039820c

Reference yield:

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 736148-55-3
N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

Guidance literature:: Multi-step reaction with 3 steps

1.1: H₂SO₄ / 24 h / 55 °C

1.2: I₂; H₂SO₄ / 5 h / 55 °C

1.3: Br₂; H₂SO₄ / 24 h / 85 °C

2.1: 66 percent / tetrakistriphenylphosphine-Pd⁽⁰⁾ / toluene / 36 h / Heating

3.1: 54 percent / pyridine; imidazole / 6 h / Heating

With pyridine; 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; In toluene; 2.1: Stille coupling;
DOI:10.1021/ja039820c

Reference yield:

: 118129-60-5
1,7-dibromoperylene-3,4,9,10-tetracarboxylic dianhydride

: 736148-55-3
N,N'-bis(4-aminophenyl)-1,7-bis(p-nitrophenyl)perylene-3,4:9,10-dicarboximide

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / tetrakistriphenylphosphine-Pd⁽⁰⁾ / toluene / 36 h / Heating

2: 54 percent / pyridine; imidazole / 6 h / Heating

With pyridine; 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; 1: Stille coupling;
DOI:10.1021/ja039820c