C₆₅H₇₉N₅O₁₂

Base Information

Chemical Name:C₆₅H₇₉N₅O₁₂
CAS No.:328267-62-5
Molecular Formula:C₆₅H₇₉N₅O₁₂
Molecular Weight:1122.37
Hs Code.:

C<sub>65</sub>H<sub>79</sub>N<sub>5</sub>O<sub>12</sub>

Synonyms:C₆₅H₇₉N₅O₁₂

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Chemical Property of C₆₅H₇₉N₅O₁₂

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Technology Process of C₆₅H₇₉N₅O₁₂

There total 18 articles about C₆₅H₇₉N₅O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 261789-05-3
4-chloro-1,8-naphthalic anhydride tert-butyl methyl benzoate

: 328267-61-4
TAC-NH₂

: 328267-62-5
C₆₅H₇₉N₅O₁₂

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; at 85 ℃; for 18h;
DOI:10.1021/ja0284761

Reference yield:

: 62819-95-8
1-(2-methoxyethoxy)-2-nitro-benzene

: 328267-62-5
C₆₅H₇₉N₅O₁₂

Guidance literature:: Multi-step reaction with 11 steps

1: 95 percent / H₂ / Pd/C / methanol / 18 h / 1672.11 Torr

2: 55 percent / K₂CO₃; KI / acetonitrile / 60 h / Heating

3: 97 percent / H₂ / Pd/C / dimethylformamide / 18 h / 1672.11 Torr

4: 69 percent / triethylamine / CH₂Cl₂ / 28 h / 20 °C

5: 61 percent / borane/THF complex / tetrahydrofuran / 2 h / Heating

6: 51 percent / pyridine / CH₂Cl₂ / 25 h / 20 °C

7: 63 percent / borane/THF complex / tetrahydrofuran / 2 h / Heating

8: 70 percent / POCl₃ / 19 h / 20 - 70 °C

9: 81 percent / ammonium acetate; acetic acid / 4 h / 55 - 60 °C

10: 51 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

11: 29 percent / diisopropylethylamine / 1-methyl-pyrrolidin-2-one / 18 h / 85 °C

With tetrahydrofuran; pyridine; ammonium acetate; lithium aluminium tetrahydride; borane; hydrogen; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja0284761

Reference yield:

: 700-38-9
2-nitro-5-methylphenol

: 328267-62-5
C₆₅H₇₉N₅O₁₂

Guidance literature:: Multi-step reaction with 11 steps

1: 50 percent / K₂CO₃ / dimethylformamide / 1 h / 120 °C

2: 55 percent / K₂CO₃; KI / acetonitrile / 60 h / Heating

3: 97 percent / H₂ / Pd/C / dimethylformamide / 18 h / 1672.11 Torr

4: 69 percent / triethylamine / CH₂Cl₂ / 28 h / 20 °C

5: 61 percent / borane/THF complex / tetrahydrofuran / 2 h / Heating

6: 51 percent / pyridine / CH₂Cl₂ / 25 h / 20 °C

7: 63 percent / borane/THF complex / tetrahydrofuran / 2 h / Heating

8: 70 percent / POCl₃ / 19 h / 20 - 70 °C

9: 81 percent / ammonium acetate; acetic acid / 4 h / 55 - 60 °C

10: 51 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

11: 29 percent / diisopropylethylamine / 1-methyl-pyrrolidin-2-one / 18 h / 85 °C

With tetrahydrofuran; pyridine; ammonium acetate; lithium aluminium tetrahydride; borane; hydrogen; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium iodide; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja0284761