sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

Base Information

Chemical Name:sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate
CAS No.:1195972-64-5
Molecular Formula:C₂₃H₂₇N₄O₅S*Na
Molecular Weight:494.547
Hs Code.:

Synonyms:sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

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Chemical Property of sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

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Technology Process of sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

There total 7 articles about sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.9%

: 1195972-61-2
4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylic acid methyl ester

: 1195972-64-5
sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

Guidance literature:: With water; sodium hydroxide; In isopropyl alcohol; at 20 - 82 ℃;

Reference yield:

: 1195972-62-3
4-(3-methanesulfonyl-propoxy)-1H-indole

: 1195972-64-5
sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; benzotriazol-1-ol / N,N-dimethyl acetamide / 20 h / 85 °C

2: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 - 80 °C

3: sodium hydroxide; water / isopropyl alcohol / 20 - 82 °C

With water; potassium carbonate; benzotriazol-1-ol; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl acetamide; isopropyl alcohol;

Reference yield:

: 2380-94-1
1H-indol-4-ol

: 1195972-64-5
sodium 4-{4-[4-(3-methanesulfonyl-propoxy)-indol-1-yl]-pyrimidin-2-ylamino}-cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate; potassium iodide / acetonitrile / 80 °C

2: potassium carbonate; benzotriazol-1-ol / N,N-dimethyl acetamide / 20 h / 85 °C

3: potassium carbonate / 1-methyl-pyrrolidin-2-one / 20 - 80 °C

4: sodium hydroxide; water / isopropyl alcohol / 20 - 82 °C

With water; potassium carbonate; benzotriazol-1-ol; potassium iodide; sodium hydroxide; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl acetamide; isopropyl alcohol; acetonitrile;