3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

Base Information

Chemical Name:3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate
CAS No.:1233941-39-3
Molecular Formula:C₂₁H₂₉O₅P
Molecular Weight:392.432
Hs Code.:

Synonyms:3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

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Chemical Property of 3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

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Technology Process of 3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

There total 2 articles about 3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 65898-11-5
(1R)-2-<(diethoxyphosphoryl)oxy>-1,7,7-trimethylbicyclo<2.2.1>hept-2-ene

: 98-88-4
benzoyl chloride

: 1233941-39-3
3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

Guidance literature:: (1R)-2-<(diethoxyphosphoryl)oxy>-1,7,7-trimethylbicyclo<2.2.1>hept-2-ene; With bis(2,2,6,6-tetramethylpiperidin-1-yl)magnesium-bis(lithium chloride) complex; In tetrahydrofuran; at 25 ℃; for 0.5h; Inert atmosphere;

With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at -20 ℃; for 0.5h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; at -20 - 25 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo100763f

Reference yield: 67.0%

: 1233941-20-2
C₁₄H₂₄BrO₄P

: 98-88-4
benzoyl chloride

: 1233941-39-3
3-benzoyl-1,7,7-trimethylbicyclo[2.2.1]hept-2-en-2-yl diethyl phosphate

Guidance literature:: C₁₄H₂₄BrO₄P; With TurboGrignard; In tetrahydrofuran; at 25 ℃; for 2h; Inert atmosphere;

With copper(I) cyanide di(lithium chloride); In tetrahydrofuran; at -20 ℃; for 0.5h; Inert atmosphere;

benzoyl chloride; In tetrahydrofuran; at -20 - 25 ℃; Inert atmosphere;
DOI:10.1021/jo100763f