[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

Base Information

Chemical Name:[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester
CAS No.:474970-84-8
Molecular Formula:C₁₇H₂₈N₂O₆
Molecular Weight:356.419
Hs Code.:

[allyloxycarbonylmethyl-(2-<i>tert</i>-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

Synonyms:[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

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Chemical Property of [allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

Chemical Property:

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Technology Process of [allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

There total 1 articles about [allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40630-84-0
allyl bromoacetate

: 57260-73-8
N-BOC-1,2-diaminoethane

: 474970-84-8
[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 25 ℃; for 20h;
DOI:10.1016/S0968-0896(02)00019-6

Reference yield:

: 474970-84-8
[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

: C₅₇H₆₅N₃O₂₁

Guidance literature:: Multi-step reaction with 7 steps

1: HCl / ethyl acetate / 10 h / 25 °C

2: 0.63 g / Huenig base / dimethylformamide / 12 h / 25 °C

3: trifluoroacetic acid / CH₂Cl₂ / 10 h / 25 °C

4: DCC / CH₂Cl₂ / 5 h / 25 °C

5: 0.24 g / triethylamine; DMAP / 15 h / 25 °C

6: 95 percent / DCC; DMAP / CH₂Cl₂ / 10 h / 25 °C

7: 75 percent / PhSiH₃ / Pd(PPh₃)4 / CH₂Cl₂ / 1 h / 25 °C

With hydrogenchloride; dmap; phenylsilane; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00019-6

Reference yield:

: 474970-84-8
[allyloxycarbonylmethyl-(2-tert-butoxycarbonylamino-ethyl)-amino]-acetic acid allyl ester

: 474971-04-5
C₇₀H₈₁N₃O₂₃

Guidance literature:: Multi-step reaction with 6 steps

1: HCl / ethyl acetate / 10 h / 25 °C

2: 0.63 g / Huenig base / dimethylformamide / 12 h / 25 °C

3: trifluoroacetic acid / CH₂Cl₂ / 10 h / 25 °C

4: DCC / CH₂Cl₂ / 5 h / 25 °C

5: 0.24 g / triethylamine; DMAP / 15 h / 25 °C

6: 95 percent / DCC; DMAP / CH₂Cl₂ / 10 h / 25 °C

With hydrogenchloride; dmap; triethylamine; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0968-0896(02)00019-6