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SB-T-1102

Base Information
  • Chemical Name:SB-T-1102
  • CAS No.:178250-27-6
  • Molecular Formula:C44H61NO15
  • Molecular Weight:843.966
  • Hs Code.:
SB-T-1102

Synonyms:SB-T-1102

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Chemical Property of SB-T-1102
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Technology Process of SB-T-1102

There total 6 articles about SB-T-1102 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h; under 760 Torr; Ambient temperature;
DOI:10.1021/jm9604080
Guidance literature:
Multi-step reaction with 4 steps
1: 1.) LiHMDS / 1.) THF, -40 deg C, 10 min, 2.) THF, from -40 to 0 deg C
2: 75 percent / LiHMDS / tetrahydrofuran / -15 - -10 °C
3: 69 percent / HF, pyridine / 5 h / 30 °C
4: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature
With pyridine; hydrogen fluoride; hydrogen; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/jm9604080
Guidance literature:
Multi-step reaction with 3 steps
1: 75 percent / LiHMDS / tetrahydrofuran / -15 - -10 °C
2: 69 percent / HF, pyridine / 5 h / 30 °C
3: 100 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature
With pyridine; hydrogen fluoride; hydrogen; lithium hexamethyldisilazane; palladium on activated charcoal; In tetrahydrofuran; ethyl acetate;
DOI:10.1021/jm9604080
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