(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

Base Information

Chemical Name:(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime
CAS No.:160925-97-3
Molecular Formula:C₂₇H₂₉NO₄
Molecular Weight:431.532
Hs Code.:

Synonyms:(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

Chemical Property:

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Technology Process of (3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

There total 2 articles about (3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 160925-97-3
(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / n-C₄H₉Li / toluene / 48 h / 40 °C

2: 1.) DCC, 2.) pyridinium trifluoroacetate, 3.) NH₂OH*HCl, KHCO₃

With n-butyllithium; hydroxylamine hydrochloride; pyridinium trifluroacetate; potassium hydrogencarbonate; dicyclohexyl-carbodiimide; In toluene;

Reference yield:

: 102208-53-7
(3R,4R,5R)-5-hydroxy-3,4,6-tribenzyloxy-1-hexene

: 160925-97-3
(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

Guidance literature:: With hydroxylamine hydrochloride; pyridinium trifluroacetate; potassium hydrogencarbonate; dicyclohexyl-carbodiimide; Yield given. Multistep reaction;

Reference yield:

: 160925-97-3
(3R,4R)-1,3,4-Tris-benzyloxy-hex-5-en-2-one oxime

: 59920-31-9
2,5-dideoxy-2,5-imino-D-mannitol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) LAH, 2.) K₂CO₃ / 1.) ether

2: 2.) KCl, 3.) I₂, HOAc

3: 100 percent / 50percent KOH / ethanol / 18 h / Heating

4: 99 percent / H₂ / Pd/C / ethanol

With potassium hydroxide; lithium aluminium tetrahydride; potassium chloride; hydrogen; iodine; potassium carbonate; acetic acid; palladium on activated charcoal; In ethanol;