2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

Base Information

Chemical Name:2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one
CAS No.:244637-74-9
Molecular Formula:C₁₉H₁₃ClIN₃O
Molecular Weight:461.689
Hs Code.:

Synonyms:2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

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Chemical Property of 2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

Chemical Property:

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Technology Process of 2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

There total 6 articles about 2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 244638-71-9
Ethyl 4-chloro-2-methyl-3-(4-nitrophenyl)-5-pyridinecarboxylate

: 244637-74-9
2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: butan-1-ol / Heating

2.1: Cu(acac)2; NaBH₄ / ethanol

3.1: isoamyl nitrite; tetrafluoroboric acid / dimethylformamide

3.2: iodine; potassium iodide / dimethylsulfoxide

With copper acetylacetonate; sodium tetrahydroborate; tetrafluoroboric acid; isopentyl nitrite; In ethanol; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1016/j.bmcl.2005.08.006

Reference yield:

: 244638-70-8
Ethyl 1,4-dihydro-2-methyl-3-(4-nitrophenyl)-4-oxo-5-pyridinecarboxylate

: 244637-74-9
2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: phosphorus oxychloride / Heating

2.1: butan-1-ol / Heating

3.1: Cu(acac)2; NaBH₄ / ethanol

4.1: isoamyl nitrite; tetrafluoroboric acid / dimethylformamide

4.2: iodine; potassium iodide / dimethylsulfoxide

With copper acetylacetonate; sodium tetrahydroborate; tetrafluoroboric acid; trichlorophosphate; isopentyl nitrite; In ethanol; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1016/j.bmcl.2005.08.006

Reference yield:

: 868363-14-8
2-{[(Z)-1-Methyl-2-(4-nitro-phenyl)-vinylamino]-methylene}-malonic acid diethyl ester

: 244637-74-9
2-(4-chlorophenyl)-2,5-dihydro-7-(4-iodophenyl)-6-methylpyrazolo[4,3-c]pyridin-3-one

Guidance literature:: Multi-step reaction with 5 steps

1.1: diphenyl ether; various solvent(s) / Heating

2.1: phosphorus oxychloride / Heating

3.1: butan-1-ol / Heating

4.1: Cu(acac)2; NaBH₄ / ethanol

5.1: isoamyl nitrite; tetrafluoroboric acid / dimethylformamide

5.2: iodine; potassium iodide / dimethylsulfoxide

With copper acetylacetonate; sodium tetrahydroborate; tetrafluoroboric acid; trichlorophosphate; isopentyl nitrite; In diphenylether; ethanol; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1016/j.bmcl.2005.08.006