2-benzyl-3-methyl-2-phenyloxirane

Base Information

• Chemical Name: 2-benzyl-3-methyl-2-phenyloxirane
• CAS No.: 56051-22-0
• Molecular Formula: C₁₆H₁₆O
• Molecular Weight: 224.302
• Mol file: 56051-22-0.mol

Synonyms:2-benzyl-3-methyl-2-phenyloxirane

Chemical Property of 2-benzyl-3-methyl-2-phenyloxirane

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-benzyl-3-methyl-2-phenyloxirane

There total 1 articles about 2-benzyl-3-methyl-2-phenyloxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1,2-diphenyl-but-2-ene (5551-45-1) → 2-benzyl-3-methyl-2-phenyloxirane (56051-22-0)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 1.33333h; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.202002844

Reference yield: 78.0%

2-benzyl-3-methyl-2-phenyloxirane (56051-22-0) → 3,4-diphenylbutan-2-ol (106026-84-0,113676-19-0,113691-44-4)

Guidance literature:

With cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; hydrogen; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; In tetrahydrofuran; at 80 ℃; for 16h; under 30003 Torr; regioselective reaction; Autoclave;

DOI:10.1002/anie.202002844

upstream raw materials:

1,2-diphenyl-but-2-ene

Downstream raw materials:

3,4-diphenylbutan-2-ol