Technology Process of 3,4-diphenylbutan-2-ol
There total 9 articles about 3,4-diphenylbutan-2-ol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
methanol;
at 20 ℃;
for 2h;
Inert atmosphere;
DOI:10.1002/adsc.201500801
- Guidance literature:
-
With
cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; hydrogen; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine];
In
tetrahydrofuran;
at 80 ℃;
for 16h;
under 30003 Torr;
regioselective reaction;
Autoclave;
DOI:10.1002/anie.202002844
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.33 h / 0 °C / Schlenk technique; Inert atmosphere
2: cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; hydrogen / tetrahydrofuran / 16 h / 80 °C / 30003 Torr / Autoclave
With
cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; hydrogen; zinc trifluoromethanesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine];
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.202002844
