3,4-diphenylbutan-2-ol

Base Information

Chemical Name:3,4-diphenylbutan-2-ol
CAS No.:106026-84-0
Molecular Formula:C₁₆H₁₈O
Molecular Weight:226.318
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-diphenylbutan-2-ol

Chemical Property:

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Technology Process of 3,4-diphenylbutan-2-ol

There total 9 articles about 3,4-diphenylbutan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 94897-34-4,54636-31-6
3,4-diphenyl-2-butanone

: 106026-84-0,113676-19-0,113691-44-4
3,4-diphenylbutan-2-ol

Guidance literature:: With sodium tetrahydroborate; In methanol; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/adsc.201500801

Reference yield: 78.0%

: 56051-22-0
2-benzyl-3-methyl-2-phenyloxirane

: 106026-84-0,113676-19-0,113691-44-4
3,4-diphenylbutan-2-ol

Guidance literature:: With cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; hydrogen; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; In tetrahydrofuran; at 80 ℃; for 16h; under 30003 Torr; regioselective reaction; Autoclave;
DOI:10.1002/anie.202002844

Reference yield:

: 5551-45-1
1,2-diphenyl-but-2-ene

: 106026-84-0,113676-19-0,113691-44-4
3,4-diphenylbutan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1.33 h / 0 °C / Schlenk technique; Inert atmosphere

2: cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; zinc trifluoromethanesulfonate; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; hydrogen / tetrahydrofuran / 16 h / 80 °C / 30003 Torr / Autoclave

With cobalt(II) bis[bis((trifluoromethyl)sulfonyl)amide]; hydrogen; zinc trifluoromethanesulfonate; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.202002844