(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

Base Information

Chemical Name:(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene
CAS No.:115513-28-5
Molecular Formula:C₁₅H₂₅NO₃
Molecular Weight:267.368
Hs Code.:

Synonyms:(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

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Chemical Property of (2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

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Technology Process of (2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

There total 6 articles about (2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 75-16-1
methylmagnesium bromide

: 115513-20-7
(2R,2'S)-2-methyl-2-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]-cyclohex-3-en-1-one

: 115513-28-5
(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

Guidance literature:: In tetrahydrofuran; diethyl ether; for 10h; Ambient temperature;
DOI:10.1021/ja00231a038

Reference yield:

: 102069-84-1
(S)-2-methoxy-1-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]benzene

: 115513-28-5
(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) potassiun, tert-butyl alcohol, ammonia / 1.) THF, -78 deg C, 2.) THF, -78 deg C, 1 h

2: 87 percent / 10percent hydrochloric acid / methanol / 24 h / Ambient temperature

3: 84 percent / tetrahydrofuran; diethyl ether / 10 h / Ambient temperature

With hydrogenchloride; ammonia; potassium; tert-butyl alcohol; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1021/ja00231a038

Reference yield:

: 102069-87-4
(2'S,6R)-1-methoxy-6-[[2'-(methoxymethyl)pyrrolidinyl]carbonyl]-6-methyl-1,4-cyclohexadiene

: 115513-28-5
(2'S,2R)-1,2-dimethyl-1-hydroxy-2-<<2'-(methoxymethyl)pyrrolidinyl>carbonyl>cyclohex-3-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 10percent hydrochloric acid / methanol / 24 h / Ambient temperature

2: 84 percent / tetrahydrofuran; diethyl ether / 10 h / Ambient temperature

With hydrogenchloride; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1021/ja00231a038