2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

Base Information

Chemical Name:2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester
CAS No.:141774-74-5
Molecular Formula:C₂₀H₂₅N₃O₃
Molecular Weight:355.437
Hs Code.:

Synonyms:2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

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Chemical Property of 2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

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Technology Process of 2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

There total 3 articles about 2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 141774-74-5
2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

Guidance literature:: N-tert-butoxycarbonyl-L-phenylalanine; With ethyl 2-(tert-butoxycarbonyloxyimino)-2-cyanoacetate; N-ethyl-N,N-diisopropylamine; In ethyl acetate; at 0 - 5 ℃; for 1h;

2-(Aminomethyl)pyridine; In ethyl acetate; at 0 - 5 ℃; for 2h;
DOI:10.1002/adsc.201200645

Reference yield: 85.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 66617-58-1
N-(tert-butoxycarbonyl)-L-phenylalanine benzyl ester

: 141774-74-5
2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

Guidance literature:: at 40 ℃; for 23h; in incubator;
DOI:10.1016/j.tetlet.2011.03.039

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 141774-74-5
2-phenyl-1-pyridin-2-ylmethylcarbamoyl ethyl carbamic acid tert butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C

2: 23 h / 40 °C / in incubator

With dmap; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tetlet.2011.03.039