3,7-dimethoxydibenzo[b,f]selenepine

Base Information

Chemical Name:3,7-dimethoxydibenzo[b,f]selenepine
CAS No.:1442110-27-1
Molecular Formula:C₁₆H₁₄O₂Se
Molecular Weight:317.246
Hs Code.:

Synonyms:3,7-dimethoxydibenzo[b,f]selenepine

Suppliers and Price of 3,7-dimethoxydibenzo[b,f]selenepine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,7-dimethoxydibenzo[b,f]selenepine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,7-dimethoxydibenzo[b,f]selenepine

There total 5 articles about 3,7-dimethoxydibenzo[b,f]selenepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 613-31-0
9,10-dihydroanthracene

: 1442110-24-8
4,8-dimethoxy-1H-dibenzo[b,f]cyclopropa[d]selenepin-1-one

: 120-12-7
anthracene

: 1442110-27-1
3,7-dimethoxydibenzo[b,f]selenepine

Guidance literature:: In toluene; at 0 ℃; Inert atmosphere; Sealed tube; Irradiation;
DOI:10.1021/ol401225n

Reference yield:

: 134953-15-4
bis(3-methoxyphenyl)selenide

: 1442110-26-0
1-benzyl-6,10-dimethoxy-1H-dibenzo[2,3:6,7]selenepino[4,5-d][1,2,3]triazole

: 1442110-27-1
3,7-dimethoxydibenzo[b,f]selenepine

Guidance literature:: Multi-step reaction with 3 steps

1.1: aluminum (III) chloride / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

1.2: -20 - 20 °C / Inert atmosphere

2.1: water / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 0 °C / Inert atmosphere; Sealed tube; Irradiation

With tetrahydrofuran; aluminum (III) chloride; water; In dichloromethane; 1.1: |Friedel-Crafts Alkylation / 1.2: |Friedel-Crafts Alkylation;
DOI:10.1021/ol401225n

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 1442110-26-0
1-benzyl-6,10-dimethoxy-1H-dibenzo[2,3:6,7]selenepino[4,5-d][1,2,3]triazole

: 1442110-27-1
3,7-dimethoxydibenzo[b,f]selenepine

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / diethyl ether / 0.17 h / 20 °C / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: aluminum (III) chloride / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

2.2: -20 - 20 °C / Inert atmosphere

3.1: water / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

4.1: tetrahydrofuran / 0 °C / Inert atmosphere; Sealed tube; Irradiation

With tetrahydrofuran; aluminum (III) chloride; n-butyllithium; water; In diethyl ether; dichloromethane; 2.1: |Friedel-Crafts Alkylation / 2.2: |Friedel-Crafts Alkylation;
DOI:10.1021/ol401225n