C₃₆H₄₅NO₃Si

Base Information Edit

Chemical Name:C₃₆H₄₅NO₃Si
CAS No.:880152-36-3
Molecular Formula:C₃₆H₄₅NO₃Si
Molecular Weight:567.844
Hs Code.:
Mol file:880152-36-3.mol

C<sub>36</sub>H<sub>45</sub>NO<sub>3</sub>Si

Synonyms:C₃₆H₄₅NO₃Si

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Chemical Property of C₃₆H₄₅NO₃Si Edit

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Technology Process of C₃₆H₄₅NO₃Si

There total 14 articles about C₃₆H₄₅NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 880152-35-2
2-[4-(tert-butyl-diphenyl-silanyloxy)-3-(6-butyl-2-oxo-2H-pyran-4-ylamino)-butyl]-cyclohex-1-enecarbaldehyde

: 880152-43-2
C₃₆H₄₅NO₃Si

: 880152-36-3
C₃₆H₄₅NO₃Si

Guidance literature:: With piperdinium acetate; sodium sulfate; In ethyl acetate; toluene; Heating;

Reference yield:

: 3-butyl-6-(tert-butyl-diphenyl-silanyloxymethyl)-5,6,7,8,9,10,11,12-octahydro-2-oxa-5-aza-dibenzo[a,d]cyclononene-1,13-dione

: 880152-43-2
C₃₆H₄₅NO₃Si

: 880152-36-3
C₃₆H₄₅NO₃Si

Guidance literature:: With piperdinium acetate; sodium sulfate; In ethyl acetate; toluene; at 150 ℃; for 12h;
DOI:10.1021/ol053059p

Reference yield:

: 880152-30-7
2-(3-tert-butoxycarbonylamino-4-hydroxy-butyl)-cyclohex-1-enecarboxylic acid ethyl ester

: 880152-36-3
C₃₆H₄₅NO₃Si

Guidance literature:: Multi-step reaction with 8 steps

1: imidazole / CH₂Cl₂ / 20 °C

2: 12.0 g / DIBAL-H / CH₂Cl₂ / -78 - 0 °C

3: pyridine / 20 °C

4: 100 percent / TFA / CH₂Cl₂ / 1 h / 0 °C

5: 61 percent / pyridine / ethanol / 48 h / Heating

6: K₂CO₃ / methanol; H₂O / 1 h / 20 °C

7: 504.0 mg / N-methylmorpholine-N-oxide; TPAP; 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h / 20 °C

8: 68 percent / Na₂SO₄; piperidinium acetate / ethyl acetate; toluene / Heating

With pyridine; 1H-imidazole; tetrapropylammonium perruthennate; 4 A molecular sieve; piperdinium acetate; diisobutylaluminium hydride; potassium carbonate; 4-methylmorpholine N-oxide; sodium sulfate; trifluoroacetic acid; In methanol; ethanol; dichloromethane; water; ethyl acetate; toluene;