(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Base Information

Chemical Name:(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester
CAS No.:185428-90-4
Molecular Formula:C₁₂H₁₆N₂O₅
Molecular Weight:268.269
Hs Code.:

Synonyms:(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Suppliers and Price of (4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of (4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

There total 7 articles about (4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 34619-03-9
tert-butyldicarbonate

: 96-96-8
4-methoxy-2-nitroaniline

: 185428-90-4
(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: 4-methoxy-2-nitroaniline; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.166667h;

tert-butyldicarbonate; In tetrahydrofuran; mineral oil; at 20 ℃; for 24h;
DOI:10.1002/chem.201402502

Reference yield: 87.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 96-96-8
4-methoxy-2-nitroaniline

: 185428-90-4
(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: 4-methoxy-2-nitroaniline; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

di-tert-butyl dicarbonate; In tetrahydrofuran; mineral oil; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/cmdc.201400040

Reference yield: 69.0%

: 18437-68-8
tert-butyl N-(4-methoxyphenyl)carbamate

: 185428-90-4
(4-methoxy-2-nitro-phenyl)-carbamic acid tert-butyl ester

Guidance literature:: With tetra-O-acetyl riboflavin; oxygen; sodium nitrite; In water; acetonitrile; at 25 ℃; Irradiation;
DOI:10.1021/acs.joc.7b03260