[Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2]

Base Information

• Chemical Name: [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2]
• CAS No.: 1154042-86-0
• Molecular Formula: C₄₆H₆₆FeO₂P₂PdS₂
• Molecular Weight: 939.375

Synonyms:[Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2]

Chemical Property of [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2]

Chemical Property:

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Technology Process of [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2]

There total 3 articles about [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4-Methoxybenzenethiol (696-63-9) + [Pd(1-dicyclohexylphopshino-2-di-tert-butylphosphinoethylferrocene)Cl2] (854019-82-2) → [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2] (1154042-86-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; N(C2H5)3, THF, room temp.;

Reference yield:

4,4'-dimethoxyphenyl disulfide (5335-87-5) + [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(p-tolyl)Br] (1154042-81-5) → [Pd(1-dicyclohexylphopshino-2-di-tert-butylphosphinoethylferrocene)Br2] (1154042-93-9) + [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)Br] (1154042-94-0,1154049-72-5) + [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2] (1154042-86-0)

Guidance literature:

In toluene; 100°C;

Reference yield:

4,4'-dimethoxyphenyl disulfide (5335-87-5) + [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(trans-stylbene)] → [Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)2] (1154042-86-0)

Guidance literature:

room temp., < 1 h;

upstream raw materials:

4,4'-dimethoxyphenyl disulfide

[Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(p-tolyl)Br]

4-Methoxybenzenethiol

[Pd(1-dicyclohexylphopshino-2-di-tert-butylphosphinoethylferrocene)Cl₂]

Downstream raw materials:

[Pd(1-dicyclohexylphopshino-2-di-tert-butylphosphinoethylferrocene)Br₂]

[Pd(1-dicyclohexylphopshino-2-di-tert-butylphosphinoethylferrocene)Cl₂]

[Pd(1-dicyclohexylphosphino-2-di-tert-butylphosphinoethylferrocene)(4-methoxybenzothiolate)Br]

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