4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

Base Information

Chemical Name:4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid
CAS No.:1379478-16-6
Molecular Formula:C₂₉H₂₆O₁₃
Molecular Weight:582.518
Hs Code.:

Synonyms:4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

Suppliers and Price of 4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

There total 1 articles about 4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 103-40-2
succinic acid monobenzyl ester

: 22888-70-6
silybin B

: 1379478-16-6
4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

Guidance literature:: succinic acid monobenzyl ester; silybin B; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;

With 5%-palladium/activated carbon; hydrogen; In ethanol; at 50 ℃; for 4h;
DOI:10.1021/jm300246n

Reference yield: 59.0%

: 1379478-16-6
4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid

: 249290-17-3
N₁-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine

: 1379505-86-8
((2S,3S)-3-(4-Hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl)-methyl 4-oxo-4-(6-(1,2,3,4-tetrahydroacridin-9-ylamino)-hexylamino)butanoate Hydrochloride

Guidance literature:: 4-(((2S,3S)-3-(4-hydroxy-3-methoxyphenyl)-6-((2R,3R)-3,5,7-trihydroxy-4-oxochroman-2-yl)-2,3-dihydrobenzo[b][1,4]dioxin-2-yl))-4-oxobutanoic Acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; toluene; at 20 ℃; for 0.5h;

N₁-(1,2,3,4-tetrahydroacridin-9-yl)hexane-1,6-diamine; In N,N-dimethyl-formamide; toluene; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jm300246n