HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH

Base Information

• Chemical Name: HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH
• CAS No.: 1351988-02-7
• Molecular Formula: C₂₆H₂₄N₄O₄
• Molecular Weight: 456.501
• Mol file: 1351988-02-7.mol

Synonyms:HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH

Chemical Property of HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH

There total 1 articles about HO₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

4-[(2-hydroxy-3-methoxy-benzylidene)-amino]-1,5-dimethyl-2-phenyl-1,2-dihydro-pyrazol-3-one (183486-17-1) + anthranilic acid (118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4) → HO2CC6H4NCN(C6H5)N(CH3)C(CH3)CNCHC6H3(OCH3)OH (1351988-02-7)

Guidance literature:

With potassium carbonate; In ethanol; for 10h; Reflux;

DOI:10.1016/j.saa.2011.09.065

Reference yield: 56.0%

HO2CC6H4NCN(C6H5)N(CH3)C(CH3)CNCHC6H3(OCH3)OH (1351988-02-7) + copper dichloride → [(O2CC6H4NCN(C6H5)N(CH3)C(CH3)CNCHC6H3(OCH3)O)Cu] (1352040-85-7)

Guidance literature:

In ethanol; soln. of chloride in EtOH was stirred with soln. of ligand in EtOH at room temp. for 2 h; concd. on H2O bath; filtered; washed (EtOH); dried (vac.); elem. anal.;

DOI:10.1016/j.saa.2011.09.065

Reference yield: 42.0%

HO2CC6H4NCN(C6H5)N(CH3)C(CH3)CNCHC6H3(OCH3)OH (1351988-02-7) + nickel dichloride (83864-14-6) → [(O2CC6H4NCN(C6H5)N(CH3)C(CH3)CNCHC6H3(OCH3)O)Ni] (1352040-86-8)

Guidance literature:

In ethanol; soln. of chloride in EtOH was stirred with soln. of ligand in EtOH at room temp. for 2 h; concd. on H2O bath; filtered; washed (EtOH); dried (vac.); elem. anal.;

DOI:10.1016/j.saa.2011.09.065

upstream raw materials:

4-[(2-hydroxy-3-methoxy-benzylidene)-amino]-1,5-dimethyl-2-phenyl-1,2-dihydro-pyrazol-3-one

anthranilic acid

Downstream raw materials:

[(O₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)O)Cu]

[(O₂CC₆H₄NCN(C₆H₅)N(CH₃)C(CH₃)CNCHC₆H₃(OCH₃)O)Ni]