4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

Base Information

Chemical Name:4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one
CAS No.:1361966-87-1
Molecular Formula:C₁₆H₂₂BClO₃
Molecular Weight:308.613
Hs Code.:

Synonyms:4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

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Technology Process of 4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

There total 3 articles about 4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 30626-03-0
(3E)-4-(4-chlorophenyl)-3-buten-2-one

: 73183-34-3
bis(pinacol)diborane

: 1361966-87-1
4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

Guidance literature:: bis(pinacol)diborane; With triphenylphosphine; copper(l) chloride; sodium t-butanolate; In tetrahydrofuran; for 0.0833333h; Inert atmosphere;

(3E)-4-(4-chlorophenyl)-3-buten-2-one; With methanol; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/chem.201102081

Reference yield:

: 3160-40-5
4-(4-chlorophenyl)-3-buten-2-one

: 73183-34-3
bis(pinacol)diborane

: 1361966-87-1
4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

Guidance literature:: bis(pinacol)diborane; With copper diacetate; (E)-2-((quinolin-8-ylimino)methyl)phenol; In diethyl ether; at 20 ℃; for 1h; Inert atmosphere;

4-(4-chlorophenyl)-3-buten-2-one; With methanol; In diethyl ether; at 20 ℃; for 15h;
DOI:10.1002/open.201800056

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 1361966-87-1
4-(4-chlorophenyl)-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)butan-2-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / methanol / 20 °C

2.1: (E)-2-((quinolin-8-ylimino)methyl)phenol; copper diacetate / diethyl ether / 1 h / 20 °C / Inert atmosphere

2.2: 15 h / 20 °C

With copper diacetate; (E)-2-((quinolin-8-ylimino)methyl)phenol; sodium hydroxide; In methanol; diethyl ether;
DOI:10.1002/open.201800056