1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

Base Information

Chemical Name:1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine
CAS No.:871976-41-9
Molecular Formula:C₁₇H₁₅ClFNS
Molecular Weight:319.83
Hs Code.:

Synonyms:1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

Suppliers and Price of 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

There total 1 articles about 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 76293-51-1
3,4-dihydro-5-phenyl-2H-1,6-benzothiazocine

: 2837-90-3
sodium 2,2-dichloro-2-fluoroacetate

: 871976-41-9
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

Guidance literature:: With N-benzyl-N,N,N-triethylammonium chloride; In dichloromethane; Heating;
DOI:10.1039/b512409c

Reference yield: 52.0%

: 871976-41-9
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

: 78-81-9
isobutylamine

: 1-isobutyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzothiazine

Guidance literature:: 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine; With zinc(II) chloride; In dichloromethane; at 20 ℃; for 0.75h;

isobutylamine; In dimethyl sulfoxide; at 100 ℃; for 0.25h; Further stages.;
DOI:10.1134/S1070428007070214

Reference yield: 52.0%

: 871976-41-9
1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine

: 100-46-9
benzylamine

: 1033192-34-5
1-benzyl-4a-phenyl-2,3,4,4a-tetrahydro-1H-pyrido[3,2-b][1,4]benzothiazine

Guidance literature:: 1-chloro-1-fluoro-1a-phenyl-1a,2,3,4-tetrahydro-1H-azirino[2,1-e][1,6]benzothiazocine; With zinc(II) chloride; In dichloromethane; at 20 ℃; for 0.75h;

benzylamine; In dimethyl sulfoxide; at 100 ℃; for 0.25h; Further stages.;
DOI:10.1134/S1070428007070214