2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride

Base Information

• Chemical Name: 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride
• CAS No.: 67485-13-6
• Molecular Formula: C₁₈H₁₈N₄*ClH
• Molecular Weight: 326.829
• Mol file: 67485-13-6.mol

Synonyms:2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride

Chemical Property of 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride

There total 2 articles about 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-aminoguanidine hydrochloride (1937-19-5,16139-18-7) + 1,5-diphenyl-1,4-pentadiene-3-one (538-58-9) → 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride (67485-13-6)

Guidance literature:

With para-dodecylbenzenesulfonic acid; In water; at 25 - 27 ℃; for 2h; Sonication;

DOI:10.1016/j.ultsonch.2012.02.009

Reference yield:

benzaldehyde (100-52-7) → 2-[3-phenyl-1-(2-phenylethenyl)-2-propen-1-ylidene]-hydrazinecarboximidamide hydrochloride (67485-13-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol; water / Sonication

2: para-dodecylbenzenesulfonic acid / water / 2 h / 25 - 27 °C / Sonication

With para-dodecylbenzenesulfonic acid; potassium hydroxide; In ethanol; water;

DOI:10.1016/j.ultsonch.2012.02.009

upstream raw materials:

1-aminoguanidine hydrochloride

1,5-diphenyl-1,4-pentadiene-3-one

benzaldehyde