1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane

Base Information

Chemical Name:1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane
CAS No.:1383675-98-6
Molecular Formula:C₃₅H₂₈O₃P₂
Molecular Weight:558.553
Hs Code.:

Synonyms:1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane

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Technology Process of 1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane

There total 1 articles about 1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.1%

: 2360-09-0
γ-diphenylphosphinopropyl alcohol

: (S)-(1,1'-binaphthyl-2,2'-dioxy)chlorophosphine

: 1383675-98-6
1-diphenylphosphino-3-{(S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-4-yloxy}propane

Guidance literature:: With triethylamine; In diethyl ether; at -10 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2dt30386h

Reference yield: 80.0%

: 35138-22-8
bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate

: 1383675-98-6
1-diphenylphosphino-1-((S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-2-yloxy)-propane

: 1383673-15-1
(1,5-cyclooctadiene)(1-diphenylphosphino-1-((S)-dinaphtho[2,1-d:1',2'-f][1,3,2]dioxaphosphepin-2-yloxy)-propane)rhodium(I) tetrafluoroborate

Guidance literature:: In dichloromethane; under Ar; soln. of P-ligand in CH2Cl2 added dropwise to soln. of Rh complex in CH2Cl2, mixt. (molar ratio = 1:1) stirred for 20 min; soln. concd., filtered, filtrate treated with Et2O;
DOI:10.1039/c2dt30386h