1-Propanol, 3-(diphenylphosphino)-

Base Information

Chemical Name:1-Propanol, 3-(diphenylphosphino)-
CAS No.:2360-09-0
Molecular Formula:C15H17OP
Molecular Weight:244.273
Hs Code.:
DSSTox Substance ID:DTXSID00448903
Nikkaji Number:J2.056.299D
Wikidata:Q82268102
Mol file:2360-09-0.mol

Synonyms:1-Propanol, 3-(diphenylphosphino)-;2360-09-0;3-diphenylphosphanylpropan-1-ol;SCHEMBL684881;3-Hydroxypropyldiphenylphosphine;DTXSID00448903

Suppliers and Price of 1-Propanol, 3-(diphenylphosphino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-Propanol, 3-(diphenylphosphino)-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:244.101702159
Heavy Atom Count:17
Complexity:177

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(CCCO)C2=CC=CC=C2

Technology Process of 1-Propanol, 3-(diphenylphosphino)-

There total 7 articles about 1-Propanol, 3-(diphenylphosphino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 343952-43-2
diphenyl-[3-(tetrahydro-pyran-2-yloxy)-propyl]-phosphane

: 2360-09-0
γ-diphenylphosphinopropyl alcohol

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 50 ℃;
DOI:10.1016/S0022-328X(00)00845-7

Reference yield: 74.0%

: 829-85-6
diphenylphosphane

: 627-30-5
1-chloro-3-hydroxypropane

: 2360-09-0
γ-diphenylphosphinopropyl alcohol

Guidance literature:: With potassium hydroxide; In dimethyl sulfoxide; at 50 ℃; for 1.5h;
DOI:10.1055/s-1986-31510

Reference yield:

: C₂₄H₂₀NO₄P

: 2360-09-0
γ-diphenylphosphinopropyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: tris(bipyridine)ruthenium(II) dichloride hexahydrate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate / N,N-dimethyl-formamide / 24 h / 20 °C / Schlenk technique; Inert atmosphere; Irradiation

2: zinc; acetic acid / tetrahydrofuran / 12 h / Schlenk technique; Inert atmosphere

With tris(bipyridine)ruthenium(II) dichloride hexahydrate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; acetic acid; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.8b01885