C₃₂H₄₆O₉Si

Base Information

Chemical Name:C₃₂H₄₆O₉Si
CAS No.:306726-26-1
Molecular Formula:C₃₂H₄₆O₉Si
Molecular Weight:602.797
Hs Code.:

C<sub>32</sub>H<sub>46</sub>O<sub>9</sub>Si

Synonyms:C₃₂H₄₆O₉Si

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Chemical Property of C₃₂H₄₆O₉Si

Chemical Property:

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Technology Process of C₃₂H₄₆O₉Si

There total 10 articles about C₃₂H₄₆O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₂O₁₀SeSi

: 306726-26-1
C₃₂H₄₆O₉Si

Guidance literature:: With vinyl acetate; diisopropylamine; In toluene; at 140 ℃; for 16h;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 306726-26-1
C₃₂H₄₆O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent / 2,6-lutidine / tetrahydrofuran / 0.5 h / -78 °C

2: 100 percent / DAST / CH₂Cl₂ / 0.5 h / 0 °C

3: SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

4: 99 percent / NaOH / methanol / 1 h / 25 °C

5: aq. NaIO₄ / NaHCO₃ / CH₂Cl₂; methanol / 2 h / 25 °C

6: iPr₂NH; vinyl acetate / toluene / 16 h / 140 °C

With 2,6-dimethylpyridine; sodium hydroxide; sodium periodate; vinyl acetate; diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; tin(ll) chloride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; toluene; 1: Etherification / 2: Rearrangement / 3: Glycosidation / 4: Debenzoylation / 5: Oxidation / 6: Cyclization;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8

Reference yield:

: 374115-40-9
phenyl 1-seleno-β-D-xylopyranoside

: 306726-26-1
C₃₂H₄₆O₉Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 51.92 g / TFA / dimethylformamide / 3 h / 45 °C

2.1: NaH / dimethylformamide / 0.08 h / 0 °C

2.2: 95 percent / nBu₄NI / dimethylformamide / 2 h / 0 - 25 °C

3.1: 96 percent / PPTS; MeOH / 1 h / 25 °C

4.1: 91 percent / 2,6-lutidine / tetrahydrofuran / 0.5 h / -78 °C

5.1: 100 percent / DAST / CH₂Cl₂ / 0.5 h / 0 °C

6.1: SnCl₂ / diethyl ether / 3 h / 0 - 25 °C

7.1: 99 percent / NaOH / methanol / 1 h / 25 °C

8.1: aq. NaIO₄ / NaHCO₃ / CH₂Cl₂; methanol / 2 h / 25 °C

9.1: iPr₂NH; vinyl acetate / toluene / 16 h / 140 °C

With 2,6-dimethylpyridine; methanol; sodium hydroxide; sodium periodate; vinyl acetate; pyridinium p-toluenesulfonate; sodium hydride; diisopropylamine; 4,4'-diaminostilbene-2,2'-disulfonic acid; trifluoroacetic acid; tin(ll) chloride; sodium hydrogencarbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene; 1.1: Cyclization / 2.1: Metallation / 2.2: Etherification / 3.1: Ring cleavage / 4.1: Etherification / 5.1: Rearrangement / 6.1: Glycosidation / 7.1: Debenzoylation / 8.1: Oxidation / 9.1: Cyclization;
DOI:10.1002/1521-3765(20000901)6:17<3116::AID-CHEM3116>3.0.CO;2-8