tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

Base Information

Chemical Name:tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate
CAS No.:1379591-89-5
Molecular Formula:C₁₈H₂₅NO₂
Molecular Weight:287.402
Hs Code.:

Synonyms:tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

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Chemical Property of tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

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Technology Process of tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

There total 8 articles about tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1379591-90-8
(2E,4E)-7-phenylhepta-2,4-dien-1-amine

: 1379591-89-5
tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 1379591-89-5
tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 1 h / -78 °C

2.1: diisobutylaluminium hydride / toluene; hexane / 6 h / -78 °C

2.2: 20 °C / pH 1

2.3: 15 h / 20 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

3.2: 1 h / -78 °C

4.1: diisobutylaluminium hydride / toluene; hexane / 3 h / -78 °C

4.2: 20 °C / pH 1 / Cooling with ice

5.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 15 h / 20 °C / Cooling with ice

6.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C

With lithium aluminium tetrahydride; diphenyl phosphoryl azide; sodium hydride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; mineral oil;

Reference yield:

: 477531-94-5
(2E,4E)-ethyl 7-phenylhepta-2,4-dienoate

: 1379591-89-5
tert-butyl [(2E,4E)-7-phenylhepta-2,4-dien-1-yl]carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / toluene; hexane / 3 h / -78 °C

1.2: 20 °C / pH 1 / Cooling with ice

2.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 15 h / 20 °C / Cooling with ice

3.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 15 h / 0 - 20 °C

With lithium aluminium tetrahydride; diphenyl phosphoryl azide; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In diethyl ether; hexane; dichloromethane; toluene;