ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Base Information

Chemical Name:ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate
CAS No.:1202576-68-8
Molecular Formula:C₂₀H₂₂Cl₂O₄
Molecular Weight:397.298
Hs Code.:

Synonyms:ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Suppliers and Price of ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Chemical Property:

Boiling Point:500.9±50.0 °C(Predicted)
Density:1.226±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

There total 4 articles about ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1202576-67-7
ethyl 3-ethoxy-3-(4-hydroxyphenyl)propionate

: 18880-04-1
3,4-dichlorobenzyl bromide

: 1202576-68-8
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Guidance literature:: With potassium carbonate; In acetone; at 20 - 60 ℃; Inert atmosphere;

Reference yield:

: 120743-99-9
p-[(tert-butyldimethylsilyl)oxy]benzaldehyde

: 1202576-68-8
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

2: silver(l) oxide / toluene / 20 - 100 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4: potassium carbonate / acetone / 20 - 60 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; silver(l) oxide; In tetrahydrofuran; acetone; toluene;

Reference yield:

: 1202576-66-6
ethyl 3-(4-{[tert-butyl(dimethyl)silyl]oxy}phenyl)-3-ethoxypropionate

: 1202576-68-8
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

2: potassium carbonate / acetone / 20 - 60 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; potassium carbonate; In tetrahydrofuran; acetone;