(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

Base Information

Chemical Name:(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid
CAS No.:1202575-32-3
Molecular Formula:C₁₈H₁₈Cl₂O₄
Molecular Weight:369.245
Hs Code.:

Synonyms:(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

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Chemical Property of (3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

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Technology Process of (3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

There total 6 articles about (3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1202575-18-5
3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

: 1202575-32-3
(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

: 1202576-85-9
(3R)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

Guidance literature:: In hexane; isopropyl alcohol; Resolution of racemate;

Reference yield:

: 1202576-68-8
ethyl 3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}3-ethoxypropionate

: 1202575-32-3
(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

: 1202576-85-9
(3R)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; water / ethanol; tetrahydrofuran / 4 h / 20 °C

2: isopropyl alcohol; hexane / Resolution of racemate

With water; sodium hydroxide; In tetrahydrofuran; ethanol; hexane; isopropyl alcohol;

Reference yield:

: 221079-70-5
ethyl 3-(4-{[tert-butyl(dimethyl)silyl]oxy}phenyl)-3-hydroxypropionate

: 1202575-32-3
(3S)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

: 1202576-85-9
(3R)-3-{4-[(3,4-dichlorobenzyl)oxy]phenyl}-3-ethoxy propanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: silver(l) oxide / toluene / 20 - 100 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

3: potassium carbonate / acetone / 20 - 60 °C / Inert atmosphere

4: sodium hydroxide; water / ethanol; tetrahydrofuran / 4 h / 20 °C

5: isopropyl alcohol; hexane / Resolution of racemate

With tetrabutyl ammonium fluoride; water; potassium carbonate; sodium hydroxide; silver(l) oxide; In tetrahydrofuran; ethanol; hexane; isopropyl alcohol; acetone; toluene;