1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

Base Information

Chemical Name:1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester
CAS No.:1312758-94-3
Molecular Formula:C₁₉H₂₄NO₄PS₂
Molecular Weight:425.51
Hs Code.:

Synonyms:1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

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Chemical Property of 1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

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Technology Process of 1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

There total 4 articles about 1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: bis(4-(methylthio)phenyl) 1-amino-2-methylpropylphosphonate hydrobromide

: 2258-42-6
formyl acetic anhydride

: 1312758-94-3
1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2010.12.008

Reference yield:

: 22945-49-9
tris(4-(methylthio)phenyl) phosphite

: 1312758-94-3
1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / 2 h / 80 °C

2: hydrogen bromide; acetic acid / 2 h / 20 °C

3: triethylamine / dichloromethane / 20 °C

With hydrogen bromide; acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.bmc.2010.12.008

Reference yield:

: 1282624-42-3
benzyl 1-(bis(4-(methylthio)phenoxy)phosphoryl)-2-methylpropylcarbamate

: 1312758-94-3
1-formamido-2-methylpropanephosphonic acid di(4-methylthiophenyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen bromide; acetic acid / 2 h / 20 °C

2: triethylamine / dichloromethane / 20 °C

With hydrogen bromide; acetic acid; triethylamine; In dichloromethane;
DOI:10.1016/j.bmc.2010.12.008