(S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

Base Information

• Chemical Name: (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one
• CAS No.: 170918-95-3
• Molecular Formula: C₁₆H₁₆N₂O₃S₂
• Molecular Weight: 348.447

Synonyms:(S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

Chemical Property of (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

Chemical Property:

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Technology Process of (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

There total 1 articles about (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenylthiomethyl chloride (7205-91-6) + (S)-(+)-4-benzyl-1,2,5-thiadiazolidin-3-one (139164-33-3) → (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ6-[1,2,5]thiadiazolidin-3-one (170918-95-3)

Guidance literature:

With triethylamine; In acetonitrile; for 20h; Heating;

DOI:10.1016/S0968-0896(98)00006-6

Reference yield: 90.0%

Cinnamyl bromide (4392-24-9) + (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ6-[1,2,5]thiadiazolidin-3-one (170918-95-3) → (S)-4-Benzyl-1,1-dioxo-5-((E)-3-phenyl-allyl)-2-phenylsulfanylmethyl-1λ6-[1,2,5]thiadiazolidin-3-one (170919-16-1)

Guidance literature:

With sodium hydride; In acetonitrile; Ambient temperature;

DOI:10.1016/S0968-0896(98)00006-6

Reference yield: 90.0%

1-bromo-butane (109-65-9) + (S)-4-Benzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ6-[1,2,5]thiadiazolidin-3-one (170918-95-3) → (S)-4-Benzyl-5-butyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ6-[1,2,5]thiadiazolidin-3-one (170919-13-8)

Guidance literature:

With sodium hydride; In acetonitrile; Ambient temperature;

DOI:10.1016/S0968-0896(98)00006-6

upstream raw materials:

phenylthiomethyl chloride

(S)-(+)-4-benzyl-1,2,5-thiadiazolidin-3-one

Downstream raw materials:

(S)-4-Benzyl-5-butyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

(S)-4-Benzyl-1,1-dioxo-5-((E)-3-phenyl-allyl)-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

(S)-4-Benzyl-5-methyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

(S)-4,5-Dibenzyl-1,1-dioxo-2-phenylsulfanylmethyl-1λ⁶-[1,2,5]thiadiazolidin-3-one

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