N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Base Information

Chemical Name:N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode
CAS No.:1104546-99-7
Molecular Formula:C₂₁H₂₂N₆O₂
Molecular Weight:390.445
Hs Code.:

Synonyms:N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

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Chemical Property of N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

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Technology Process of N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

There total 5 articles about N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 615-18-9
2-chloro-1,3-benzoxazole

: 1104546-98-6
2-{ethyl-[5-methyl-2-(2H-1,2,3-triazol-2-yl)benzoyl]amino}aethanaminium chloride

: 1104546-99-7
N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 52548-14-8
2-iodoyl-5-methylbenzoic acid

: 1104546-99-7
N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: Multi-step reaction with 5 steps

1: caesium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

2: thionyl chloride / dichloromethane / 1 h / 20 °C

3: triethylamine / tetrahydrofuran / 0.75 h / 20 °C

4: hydrogenchloride / ethyl acetate / 0.25 h

5: triethylamine / N,N-dimethyl-formamide / 20 °C

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; hydrogenchloride; copper(l) iodide; thionyl chloride; caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 956317-36-5
2-(2H-1,2,3-triazol-2-yl)-5-methylbenzoic acid

: 1104546-99-7
N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / dichloromethane / 1 h / 20 °C

2: triethylamine / tetrahydrofuran / 0.75 h / 20 °C

3: hydrogenchloride / ethyl acetate / 0.25 h

4: triethylamine / N,N-dimethyl-formamide / 20 °C

With hydrogenchloride; thionyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;