N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Base Information

Chemical Name:N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode
CAS No.:1104547-00-3
Molecular Formula:C₂₂H₂₄N₆O₂
Molecular Weight:404.472
Hs Code.:

Synonyms:N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

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Chemical Property of N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Chemical Property:

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Technology Process of N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

There total 5 articles about N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1104546-99-7
N-[2-(1,3-benzoxazol-2-ylamino)ethyl]-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

: 74-88-4
methyl iodide

: 1104547-00-3
N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

Reference yield:

: 52548-14-8
2-iodoyl-5-methylbenzoic acid

: 1104547-00-3
N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: Multi-step reaction with 6 steps

1: caesium carbonate; copper(l) iodide; trans-N,N'-dimethyl-1,2-cyclohexyldiamine / N,N-dimethyl-formamide / 0.17 h / 120 °C / Microwave irradiation

2: thionyl chloride / dichloromethane / 1 h / 20 °C

3: triethylamine / tetrahydrofuran / 0.75 h / 20 °C

4: hydrogenchloride / ethyl acetate / 0.25 h

5: triethylamine / N,N-dimethyl-formamide / 20 °C

6: sodium hydride / N,N-dimethyl-formamide / 0.17 h

With trans-N,N'-dimethyl-1,2-cyclohexyldiamine; hydrogenchloride; copper(l) iodide; thionyl chloride; sodium hydride; caesium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 956317-36-5
2-(2H-1,2,3-triazol-2-yl)-5-methylbenzoic acid

: 1104547-00-3
N-{2-[1,3-benzoxazol-2-yl(methyl)amino]ethyl}-N-ethyl-5-methyl-2-(2H-1,2,3-triazol-2-yl)benzamode

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / dichloromethane / 1 h / 20 °C

2: triethylamine / tetrahydrofuran / 0.75 h / 20 °C

3: hydrogenchloride / ethyl acetate / 0.25 h

4: triethylamine / N,N-dimethyl-formamide / 20 °C

5: sodium hydride / N,N-dimethyl-formamide / 0.17 h

With hydrogenchloride; thionyl chloride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;