(cyclopentadienyl)TiCl(OPh)2

Base Information

Chemical Name:(cyclopentadienyl)TiCl(OPh)2
CAS No.:36496-76-1
Molecular Formula:C₁₇H₁₅ClO₂Ti
Molecular Weight:334.638
Hs Code.:

Synonyms:(cyclopentadienyl)TiCl(OPh)2

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Chemical Property of (cyclopentadienyl)TiCl(OPh)2

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Technology Process of (cyclopentadienyl)TiCl(OPh)2

There total 3 articles about (cyclopentadienyl)TiCl(OPh)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 108-95-2,27073-41-2
phenol

: 36496-76-1
(cyclopentadienyl)TiCl(OPh)2

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; lithium nitride; In tetrahydrofuran; byproducts: (CH3)4C5H6NOH*HCl; Ti-contg. compd. (1 mmol) and Li3N (0.33 mmol) were mixed in THF and stirred for 10 min until the color changed to green; th this mixt. was added 2,2,6,6-tetramethyl-1-piperidinyloxy radical (1 mmol) in THF; after 10min, alc. (2 mmol) was added; after stiiring for 30 min, THF was removed in vac.; extn. in pentane, filtration and evacuation of the resulting yellow soln.;
DOI:10.1039/b314027j

Reference yield: 68.8%

: 1270-98-0
cyclopentadienyl titanium(IV) trichloride

: 12149-47-2
CpTi(OPh)3

: 36496-76-1
(cyclopentadienyl)TiCl(OPh)2

Guidance literature:: In hexane; under N2, CpTi(OPh)3 in hexane added to slurry of CpTiCl3 in hexane, stirred for 2 h; evapd. in vac., recrystd. (n-hexane); elem. anal.;
DOI:10.1039/DT9820000271