(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

Base Information

Chemical Name:(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride
CAS No.:122314-40-3
Molecular Formula:C₂₈H₃₈N₄O₅*ClH
Molecular Weight:547.094
Hs Code.:

Synonyms:(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

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Chemical Property of (benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

Chemical Property:

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Technology Process of (benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

There total 7 articles about (benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32393-52-5
N^α-(benzyloxycarbonyl)-N^δ-(tert-butoxycarbonyl)-L-ornithine methyl ester

: 122314-40-3
(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: diisobutylaluminum hydride (DIBAL) / toluene; hexane / 3 h / -50 °C

2: sodium acetate / ethanol; H₂O / 0.75 h / Heating

3: 76 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

4: triethylamine / CHCl₃ / 3 h / 0 °C

5: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; sodium acetate; diisobutylaluminium hydride; triethylamine; palladium on activated charcoal; In methanol; ethanol; hexane; chloroform; water; toluene;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-14-1
((S)-4-tert-Butoxycarbonylamino-1-formyl-butyl)-carbamic acid benzyl ester

: 122314-40-3
(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / ethanol; H₂O / 0.75 h / Heating

2: 76 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

3: triethylamine / CHCl₃ / 3 h / 0 °C

4: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; sodium acetate; triethylamine; palladium on activated charcoal; In methanol; ethanol; chloroform; water;
DOI:10.1021/jm00163a014

Reference yield:

: 122314-19-6
N^α-(benzyloxycarbonyl)-N^δ-(tert-butoxycarbonyl)-L-ornithinal semicarbazone

: 122314-40-3
(benzyloxycarbonyl)-L-leucyl-L-phenylalanyl-L-ornithinal hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / H₂, 1 M hydrochloric acid / 10percent Pd/C / methanol / 3.5 h

2: triethylamine / CHCl₃ / 3 h / 0 °C

3: 1.) 37percent formalin, 0.1 M hydrochloric acid, 2.) 4 M hydrochloric acid / 1.) methanol, 0 deg C, 2 h, 2.) dioxane, 0 deg C, 3 h

With hydrogenchloride; formaldehyd; hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1021/jm00163a014