C₃₂H₂₄N₂O₄S

Base Information

Chemical Name:C₃₂H₂₄N₂O₄S
CAS No.:1620070-37-2
Molecular Formula:C₃₂H₂₄N₂O₄S
Molecular Weight:532.62
Hs Code.:

C<sub>32</sub>H<sub>24</sub>N<sub>2</sub>O<sub>4</sub>S

Synonyms:C₃₂H₂₄N₂O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₂₄N₂O₄S

Chemical Property:

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Technology Process of C₃₂H₂₄N₂O₄S

There total 7 articles about C₃₂H₂₄N₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₂₆N₂O₄S

: 1620070-37-2
C₃₂H₂₄N₂O₄S

Guidance literature:: With lithium hydroxide monohydrate; at 20 ℃;

Reference yield:

: 6602-54-6
2-chloro-3-pyridinecarbonitrile

: 1620070-37-2
C₃₂H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium methylate / N,N-dimethyl-formamide / 24 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 5 h / Reflux

3.1: sodium methylate / N,N-dimethyl-formamide / 0 - 20 °C

4.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

5.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

6.1: triethylamine; dmap / 1,2-dichloro-ethane / 0.25 h / 0 °C

6.2: 0.17 h / 0 °C

6.3: 2 h / 20 °C / Inert atmosphere

7.1: lithium hydroxide monohydrate / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium hydroxide monohydrate; sodium methylate; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 1620074-99-8
C₉H₆N₂S

: 1620070-37-2
C₃₂H₂₄N₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 1 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 8 h / 60 °C

3.1: triethylamine; dmap / 1,2-dichloro-ethane / 0.25 h / 0 °C

3.2: 0.17 h / 0 °C

3.3: 2 h / 20 °C / Inert atmosphere

4.1: lithium hydroxide monohydrate / 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; lithium hydroxide monohydrate; potassium carbonate; triethylamine; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;