all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)]

Base Information

• Chemical Name: all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)]
• CAS No.: 261528-44-3
• Molecular Formula: C₅₀H₄₄N₂O₁₀P₂S₄Sn
• Molecular Weight: 1141.83

Synonyms:all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)]

Chemical Property of all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)]

Chemical Property:

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Technology Process of all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)]

There total 1 articles about all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

di-μ-hydroxo-bis[(benzene-1,2-disulfonimido)dimethyl-tin(IV)] + Triphenylphosphine oxide (791-28-6) → all-trans-[dimethyl-bis(benzene-1,2-disulfonylamido-O)-bis(triphenylphosphane oxid-O)tin(IV)] (261528-44-3) + dimethyltin oxide (2273-45-2)

Guidance literature:

In acetonitrile; byproducts: H2O; addn. of PPh3O to suspn. of Sn-compd. in MeCN, stirring for 4 h under boiling; Me2SnO was filtered off from hot soln., evapn. at 20°C, digested with Et2O, recrystn. from hot MeCN and slow cooling to -20°C; elem. anal.;

DOI:10.1002/(sici)1521-3749(200002)626:2<529::aid-zaac529>3.0.co;2-v

upstream raw materials:

Triphenylphosphine oxide

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