C₃₁H₁₉Cl₂F₃N₂O₅

Base Information

Chemical Name:C₃₁H₁₉Cl₂F₃N₂O₅
CAS No.:1443038-26-3
Molecular Formula:C₃₁H₁₉Cl₂F₃N₂O₅
Molecular Weight:627.403
Hs Code.:

C<sub>31</sub>H<sub>19</sub>Cl<sub>2</sub>F<sub>3</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₁H₁₉Cl₂F₃N₂O₅

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Chemical Property of C₃₁H₁₉Cl₂F₃N₂O₅

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Technology Process of C₃₁H₁₉Cl₂F₃N₂O₅

There total 12 articles about C₃₁H₁₉Cl₂F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.5%

: 1443038-16-1
C₃₁H₂₁Cl₂F₃N₂O₆

: 1443038-26-3
C₃₁H₁₉Cl₂F₃N₂O₅

Guidance literature:: With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 3h;
DOI:10.1016/j.ejmech.2013.02.040

Reference yield:

: 2040-90-6
2-chloro-6-fluorophenol

: 1443038-26-3
C₃₁H₁₉Cl₂F₃N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / dichloromethane / 3 h / 0 - 20 °C

2: aluminum (III) chloride / 1 h / 150 °C

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C

4: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

5: 2,6-dimethylpyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 12 h / 20 °C

6: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 3 h / 0 °C

With pyridine; 2,6-dimethylpyridine; aluminum (III) chloride; trifluoromethylsulfonic anhydride; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2: |Fries Phenol Ester Rearrangement;
DOI:10.1016/j.ejmech.2013.02.040

Reference yield:

: 1443037-87-3
2-chloro-6-fluorophenyl-4-fluorobenzoate

: 1443038-26-3
C₃₁H₁₉Cl₂F₃N₂O₅

Guidance literature:: Multi-step reaction with 5 steps

1: aluminum (III) chloride / 1 h / 150 °C

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 60 °C

3: sodium hydroxide; water / tetrahydrofuran / 1 h / 20 °C

4: 2,6-dimethylpyridine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dichloromethane / 12 h / 20 °C

5: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 3 h / 0 °C

With pyridine; 2,6-dimethylpyridine; aluminum (III) chloride; trifluoromethylsulfonic anhydride; water; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; sodium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: |Fries Phenol Ester Rearrangement;
DOI:10.1016/j.ejmech.2013.02.040