3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine

Base Information

• Chemical Name: 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine
• CAS No.: 52417-09-1
• Molecular Formula: C₅₂H₅₀N₂O₉
• Molecular Weight: 846.977

Synonyms:3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine

Chemical Property of 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine

Chemical Property:

Purity/Quality:

95-1122%min ^*data from raw suppliers

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Technology Process of 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine

There total 6 articles about 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4) → 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine (52417-09-1)

Guidance literature:

at 70 ℃;

DOI:10.1021/tx060032l

Reference yield: 93.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + thymidine (50-89-5,28854-96-8,3545-96-8,50-88-4) → 5'-O-(4-4'-dimethoxytrityl)thymidine (40615-39-2) + 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine (52417-09-1)

Guidance literature:

With pyridine; at 20 ℃; for 1.5h;

DOI:10.1080/15257770600726059

Reference yield: 93.0%

4,4'-dimethoxytrityl chloride (40615-36-9) + C10H14N2O5 (50-89-5,3424-98-4,4449-43-8,4781-17-3,16053-52-4,36646-86-3,39131-66-3,68224-82-8,128112-70-9,131682-41-2,137121-87-0,28854-96-8,3545-96-8,50-88-4) → 5'-O-(4-4'-dimethoxytrityl)thymidine (40615-39-2) + 3'-O-(4,4'-dimethoxytriphenylmethyl)-5'-O-fluorenylmethoxycarbonylthymidine (52417-09-1)

Guidance literature:

With pyridine; at 20 ℃; for 0.5h;

upstream raw materials:

4,4'-dimethoxytrityl chloride

thymidine

1,2,3-triazole

3'-O-trimethylsilyl-5'-O-dimethoxytrityl-thymidine

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