methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside
CAS No.:1352299-27-4
Molecular Formula:C₄₅H₄₄F₁₃NO₉
Molecular Weight:989.825
Hs Code.:

Synonyms:methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

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Chemical Property of methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

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Technology Process of methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

There total 5 articles about methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₄₅NO₈

: 52447-22-0
perfluoroheptanoyl chloride

: 1352299-27-4
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h;
DOI:10.1016/j.tet.2011.09.030

Reference yield:

: C₁₅H₂₁N₃O₄

: 1352299-27-4
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: camphor-10-sulfonic acid / tetrahydrofuran; methanol / 0.08 h / 20 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 70 °C

3: ammonium chloride; zinc / tetrahydrofuran; water / 0.17 h / 0 - 20 °C

4: triethylamine / tetrahydrofuran; water / 2 h / 0 - 20 °C

With camphor-10-sulfonic acid; sodium hydride; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.030

Reference yield:

: 1352299-25-2
4-[2-(2-azidoethoxy)ethoxy]phenol

: 1352299-27-4
methyl 2,3,4-tri-O-benzyl-6-O-{4-[2-(2-(tridecafluorohexanecarboxamido)ethoxy)ethoxy]phenyl}-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 3 h / 70 °C

2: ammonium chloride; zinc / tetrahydrofuran; water / 0.17 h / 0 - 20 °C

3: triethylamine / tetrahydrofuran; water / 2 h / 0 - 20 °C

With sodium hydride; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2011.09.030