C₂₂H₃₀O₅

Base Information

• Chemical Name: C₂₂H₃₀O₅
• CAS No.: 1028432-69-0
• Molecular Formula: C₂₂H₃₀O₅
• Molecular Weight: 374.477
• Mol file: 1028432-69-0.mol

Synonyms:C₂₂H₃₀O₅

Chemical Property of C₂₂H₃₀O₅

Chemical Property:

Purity/Quality:

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Technology Process of C₂₂H₃₀O₅

There total 1 articles about C₂₂H₃₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

[(2R,3R)-3-[4-(benzyloxy)butyl]oxiran-2-yl]methanol (99095-30-4) + 4-Methoxybenzyl alcohol (105-13-5) → C22H30O5 (1028432-69-0)

Guidance literature:

4-Methoxybenzyl alcohol; With titanium(IV) isopropylate; at 100 ℃; for 0.5h; Inert atmosphere;

[(2R,3R)-3-[4-(benzyloxy)butyl]oxiran-2-yl]methanol; In toluene; at 85 ℃; for 1.25h; Inert atmosphere;

With sulfuric acid; water; In diethyl ether; toluene; at 20 ℃; for 3h; regioselective reaction;

DOI:10.1021/ol800685c

Reference yield:

2-mesitylenesulphonyl chloride (773-64-8) + C22H30O5 (1028432-69-0) → C31H40O7S

Guidance literature:

With pyridine; In dichloromethane; at 0 - 20 ℃; chemoselective reaction; Inert atmosphere;

DOI:10.1021/ol800685c

upstream raw materials:

[(2R,3R)-3-[4-(benzyloxy)butyl]oxiran-2-yl]methanol

4-Methoxybenzyl alcohol