[1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol

Base Information

• Chemical Name: [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol
• CAS No.: 134262-35-4
• Molecular Formula: C₃₂H₃₅NO₄
• Molecular Weight: 497.634

Synonyms:[1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol

Chemical Property of [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol

Chemical Property:

Purity/Quality:

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Technology Process of [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol

There total 1 articles about [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(1S,3S)-2-Benzyl-7-(2-hydroxymethyl-4,5-dimethoxy-naphthalen-1-yl)-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-8-ol (129437-12-3) + dimethyl sulfate (77-78-1) → [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol (134262-35-4)

Guidance literature:

With sodium hydroxide; benzyltri(n-butyl)ammonium chloride; In dichloromethane; for 0.333333h;

Reference yield: 86.0%

succinic acid anhydride (108-30-5) + [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol (134262-35-4) → 3-<1-<(1S,3S,7R)-2-benzyl-1,2,3,4-tetrahydro-8-methoxy-1,3-dimethyl-7-isoquinolyl>-4,5-dimethoxy-2-naphthylmethyloxycarbonyl>propanoic acid hydrochloride (134354-89-5)

Guidance literature:

With dmap; triethylamine; for 5h;

Reference yield:

succinic acid anhydride (108-30-5) + [1-((1S,3S)-2-Benzyl-8-methoxy-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-7-yl)-4,5-dimethoxy-naphthalen-2-yl]-methanol (134262-35-4) → 3-<1-<(1S,3S,7S)-2-benzyl-1,2,3,4-tetrahydro-8-methoxy-1,3-dimethyl-7-isoquinolyl>-4,5-dimethoxy-2-naphthylmethyloxycarbonyl>propanoic acid hydrochloride (134262-36-5)

Guidance literature:

With dmap; triethylamine; Yield given;

upstream raw materials:

(1S,3S)-2-Benzyl-7-(2-hydroxymethyl-4,5-dimethoxy-naphthalen-1-yl)-1,3-dimethyl-1,2,3,4-tetrahydro-isoquinolin-8-ol

dimethyl sulfate

Downstream raw materials:

3-<1-<(1S,3S,7S)-2-benzyl-1,2,3,4-tetrahydro-8-methoxy-1,3-dimethyl-7-isoquinolyl>-4,5-dimethoxy-2-naphthylmethyloxycarbonyl>propanoic acid hydrochloride

3-<1-<(1S,3S,7R)-2-benzyl-1,2,3,4-tetrahydro-8-methoxy-1,3-dimethyl-7-isoquinolyl>-4,5-dimethoxy-2-naphthylmethyloxycarbonyl>propanoic acid hydrochloride

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