1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

Base Information

Chemical Name:1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole
CAS No.:1201688-22-3
Molecular Formula:C₁₉H₁₈N₄S
Molecular Weight:334.445
Hs Code.:

Synonyms:1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

Chemical Property:

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Technology Process of 1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

There total 6 articles about 1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2360-22-7
1-methyl-1,3-dihydro-2H-benzimidazole-2-thione

: 1201687-66-2
2-chloromethyl-1-methyl-4-phenyl-1H-imidazole

: 1201688-22-3
1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 90 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 675148-45-5
(1-methyl-4-phenyl-1H-imidazol-2-yl)methanol

: 1201688-22-3
1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 90 °C / Microwave irradiation

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 911719-02-3
methyl 1-methyl-4-phenyl-1H-imidazole-2-carboxylate

: 1201688-22-3
1-methyl-2-(1-methyl-4-phenyl-1H-imidazol-2-ylmethylsulfanyl)-1H-benzoimidazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / -10 - -5 °C / Inert atmosphere

1.2: 0 °C / pH 6

2.1: thionyl chloride / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 90 °C / Microwave irradiation

With lithium aluminium tetrahydride; thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;