methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Base Information

Chemical Name:methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate
CAS No.:877286-53-8
Molecular Formula:C₂₅H₂₇NO₃
Molecular Weight:389.494
Hs Code.:

Synonyms:methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

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Chemical Property of methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

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Technology Process of methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

There total 3 articles about methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 877286-38-9
methyl 13-cyclohexyl-6-oxo-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

: 877286-53-8
methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

Reference yield:

: 885479-25-4
methyl 10-cyclohexyl-2-oxo-3a,14b-dihydro-4H[1,3]dioxolo[4,5-d]indolo[2,1-a][2]benzazepine-7-carboxylate

: 877286-53-8
methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: With hydrogen; nickel; In methanol; water; acetone; for 48h; under 760.051 Torr;
DOI:10.1055/s-0029-1217168

Reference yield:

: 877267-61-3
methyl 13-cyclohexyl-7H-indolo[2,1-a][2]benzazepine-10-carboxylate

: 877286-53-8
methyl 13-cyclohexyl-6-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

: 1178564-69-6
methyl 13-cyclohexyl-5-hydroxy-6,7-dihydro-5H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: methyl 13-cyclohexyl-7H-indolo[2,1-a][2]benzazepine-10-carboxylate; With dimethylsulfide borane complex; In tetrahydrofuran; at 20 ℃; for 2h;

With water; dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1055/s-0029-1217168