C₅₂H₇₄N₂O₁₀Si₃

Base Information

Chemical Name:C₅₂H₇₄N₂O₁₀Si₃
CAS No.:1410805-50-3
Molecular Formula:C₅₂H₇₄N₂O₁₀Si₃
Molecular Weight:971.423
Hs Code.:

C<sub>52</sub>H<sub>74</sub>N<sub>2</sub>O<sub>10</sub>Si<sub>3</sub>

Synonyms:C₅₂H₇₄N₂O₁₀Si₃

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Chemical Property of C₅₂H₇₄N₂O₁₀Si₃

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Technology Process of C₅₂H₇₄N₂O₁₀Si₃

There total 23 articles about C₅₂H₇₄N₂O₁₀Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₂H₇₃BrN₂O₁₀Si₃

: 1410805-50-3
C₅₂H₇₄N₂O₁₀Si₃

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol302691j

Reference yield:

: C₂₈H₄₉NO₇Si₂

: 1410805-50-3
C₅₂H₇₄N₂O₁₀Si₃

Guidance literature:: Multi-step reaction with 5 steps

1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.2 h / 20 °C / pH 7 / Inert atmosphere

2: hydroxylamine hydrochloride; pyridine / ethanol / 2.5 h / 0 °C / Inert atmosphere

3: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44 h / 20 - 50 °C / Inert atmosphere

4: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: samarium diiodide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

With pyridine; sodium periodate; N-chloro-succinimide; samarium diiodide; hydroxylamine hydrochloride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; aq. phosphate buffer; ethanol; dichloromethane; chloroform; 5: |Reformatsky Reaction;
DOI:10.1021/ol302691j

Reference yield:

: C₂₇H₄₅NO₆Si₂

: 1410805-50-3
C₅₂H₇₄N₂O₁₀Si₃

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; pyridine / ethanol / 2.5 h / 0 °C / Inert atmosphere

2: pyridine; N-ethyl-N,N-diisopropylamine; N-chloro-succinimide / chloroform / 44 h / 20 - 50 °C / Inert atmosphere

3: Dess-Martin periodane / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: samarium diiodide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

With pyridine; N-chloro-succinimide; samarium diiodide; hydroxylamine hydrochloride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; chloroform; 4: |Reformatsky Reaction;
DOI:10.1021/ol302691j