Technology Process of C22H32N2O
There total 5 articles about C22H32N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1021/jo102124d
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 20 h / 60 °C
2: sodium tetrahydroborate; nickel dichloride / methanol / -60 - -30 °C
3: dicyclohexyl-carbodiimide / dichloromethane / 2.5 h / 20 °C
4: palladium 10% on activated carbon; hydrogen / methanol / 20 °C
5: triethylamine / tetrahydrofuran / 0 - 20 °C
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydroxylamine hydrochloride; hydrogen; sodium acetate; triethylamine; dicyclohexyl-carbodiimide; nickel dichloride;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water;
DOI:10.1021/jo102124d
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium tetrahydroborate; nickel dichloride / methanol / -60 - -30 °C
2: dicyclohexyl-carbodiimide / dichloromethane / 2.5 h / 20 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 20 °C
4: triethylamine / tetrahydrofuran / 0 - 20 °C
With
sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; triethylamine; dicyclohexyl-carbodiimide; nickel dichloride;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo102124d
