1-[(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)methyl]-1H-1,2,3-benzotriazole

Base Information

Chemical Name:1-[(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)methyl]-1H-1,2,3-benzotriazole
CAS No.:122503-12-2
Molecular Formula:C₁₇H₁₃N₇S
Molecular Weight:347.403
Hs Code.:
Mol file:122503-12-2.mol

Synonyms:6-benzyl-3-<1-(1H-benzotriazole)methyl>-1,2,4-triazolo<3,4-b><1,3,4>thiadiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)methyl]-1H-1,2,3-benzotriazole

Chemical Property:

Melting Point:158-159 °C(Solv: ethanol (64-17-5))
PKA:1.29±0.30(Predicted)
Density:1.55±0.1 g/cm3(Predicted)

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of 1-[(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)methyl]-1H-1,2,3-benzotriazole

There total 4 articles about 1-[(6-benzyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazol-3-yl)methyl]-1H-1,2,3-benzotriazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 103-82-2
phenylacetic acid

: 122503-09-7
1-(4-amino-4H-1,2,4-triazole-3-thion-5-yl)methyl-1H-benzotriazole

: 122503-12-2
6-benzyl-3-<1-(1H-benzotriazole)methyl>-1,2,4-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: With trichlorophosphate; at 90 ℃; for 0.5h;
DOI:10.1002/jhet.5570260131

Reference yield:

: 69218-46-8
ethyl (1H-benzotriazol-1-yl)acetate

: 122503-12-2
6-benzyl-3-<1-(1H-benzotriazole)methyl>-1,2,4-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / hydrazine hydrate / ethanol / 1 h / Heating

2: potassium hydroxide / ethanol / 16 h / Ambient temperature

3: 70percent aq. hydrazine hydrate / 2 h / Heating

4: 81 percent / POCl₃ / 0.5 h / 90 °C

With potassium hydroxide; hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1002/jhet.5570260131

Reference yield:

: 122502-94-7
2-(1H-benzo[d][1,2,3]triazol-1-yl)acetohydrazide

: 122503-12-2
6-benzyl-3-<1-(1H-benzotriazole)methyl>-1,2,4-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol / 16 h / Ambient temperature

2: 70percent aq. hydrazine hydrate / 2 h / Heating

3: 81 percent / POCl₃ / 0.5 h / 90 °C

With potassium hydroxide; hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1002/jhet.5570260131