Technology Process of 5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester
There total 4 articles about 5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
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1358816-97-3
5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester
- Guidance literature:
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With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 0 - 20 ℃;
DOI:10.1039/c1nj20530g
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1358816-97-3
5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 0 - 25 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
With
tetrabutyl ammonium fluoride; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1039/c1nj20530g
-
-
1358816-97-3
5-hydroxy-isophthalic acid bis-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl) ester
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid / tetrahydrofuran; water / 3 h
2: 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide / tetrahydrofuran; dichloromethane / 0 - 25 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C
With
tetrabutyl ammonium fluoride; 4-pyrrolidin-1-ylpyridine; acetic acid; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1039/c1nj20530g
