N,N',5',6'-tetramethyl-N,N'-bis

Base Information

Chemical Name:N,N',5',6'-tetramethyl-N,N'-bis
CAS No.:156818-65-4
Molecular Formula:C₂₉H₂₆N₆O₆
Molecular Weight:554.562
Hs Code.:

N,N',5',6'-tetramethyl-N,N'-<methylenebis(2-nitrophen-4,1-ylene)>bis<pyridine-2-carboxamide>

Synonyms:N,N',5',6'-tetramethyl-N,N'-bis

Suppliers and Price of N,N',5',6'-tetramethyl-N,N'-bis

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N,N',5',6'-tetramethyl-N,N'-bis

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of N,N',5',6'-tetramethyl-N,N'-bis

There total 4 articles about N,N',5',6'-tetramethyl-N,N'-bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 128073-07-4
5-methylpyridine-2-carboxylic acid chloride

: 156818-62-1
N,6-dimethyl-N-<4'-<4''-(methylamino)-3''-nitrobenzyl>-2'-nitrophenyl>pyridine-2-carboxamide

: 156818-65-4
N,N',5',6'-tetramethyl-N,N'-bis

Guidance literature:: With triethylamine; In chloroform; for 15h; Ambient temperature;
DOI:10.1002/hlca.19940770406

Reference yield:

: 126125-54-0
6-methyl-pyridine-2-carbonyl chloride

: 156818-65-4
N,N',5',6'-tetramethyl-N,N'-bis

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / Et₃N / CHCl₃ / 15 h / Ambient temperature

2: 88 percent / Et₃N / CHCl₃ / 15 h / Ambient temperature

With triethylamine; In chloroform;
DOI:10.1002/hlca.19940770406

Reference yield:

: 4434-13-3
2-carboxy-5-methylpyridine

: 156818-65-4
N,N',5',6'-tetramethyl-N,N'-bis

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / dimethylformamide / 1.5 h / Heating

2: 88 percent / Et₃N / CHCl₃ / 15 h / Ambient temperature

With thionyl chloride; triethylamine; In chloroform; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19940770406