tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

Base Information

Chemical Name:tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate
CAS No.:302341-66-8
Molecular Formula:C₁₉H₂₄N₄O₂S
Molecular Weight:372.491
Hs Code.:

Synonyms:tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

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Chemical Property of tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

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Technology Process of tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

There total 2 articles about tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 94838-55-8
tert-butyl (4-aminobenzyl)carbamate

: 302341-66-8
tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

Guidance literature:: 1,1'-Thiocarbonyldiimidazole; tert-butyl (4-aminobenzyl)carbamate; With 1H-imidazole; In acetonitrile; at 20 ℃; for 2h;

1,2-diamino-benzene; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/S0968-0896(02)00616-8

Reference yield:

: C₁₆H₂₂N₄O₂S

: 95-54-5
1,2-diamino-benzene

: 302341-66-8
tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

Guidance literature:: at 20 ℃;
DOI:10.1016/j.bmcl.2009.07.016

Reference yield:

: 302341-66-8
tert-butyl 4-({[(2-aminophenyl)amino]carbonothioyl}amino)benzylcarbamate

: N-[4-(aminomethyl)phenyl]-1H-benzimidazol-2-amine bishydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / yellow HgO; sulfur / ethanol / 2 h / Heating

2: 90.8 percent / HCl / CH₂Cl₂; diethyl ether / 2 h / 20 °C

With hydrogenchloride; sulfur; mercury(II) oxide; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/S0968-0896(02)00616-8