BOC-L-4-BR-PHE-NH2

Base Information

Chemical Name:BOC-L-4-BR-PHE-NH2
CAS No.:869569-99-3
Molecular Formula:C₁₄H₁₉BrN₂O₃
Molecular Weight:343.22
Hs Code.:
Mol file:869569-99-3.mol

Synonyms:Carbamicacid, [(1S)-2-amino-1-[(4-bromophenyl)methyl]-2-oxoethyl]-, 1,1-dimethylethylester (9CI); (2S)-2-(tert-Butoxycarbonylamino)-3-(4-bromophenyl)propanamide

Suppliers and Price of BOC-L-4-BR-PHE-NH2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
BOC-L-4-BR-PHE-NH2 95.00%
5G
$ 1617.00

American Custom Chemicals Corporation
BOC-L-4-BR-PHE-NH2 95.00%
1G
$ 866.25

Total 14 raw suppliers

Chemical Property of BOC-L-4-BR-PHE-NH2

Chemical Property:

Boiling Point:526.7 °C at 760 mmHg
Flash Point:272.3 °C
PSA：81.42000
Density:1.367
LogP:3.46140

Purity/Quality:

98%,99%, ^*data from raw suppliers

BOC-L-4-BR-PHE-NH2 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of BOC-L-4-BR-PHE-NH2

There total 6 articles about BOC-L-4-BR-PHE-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.6%

: 266306-18-7
(S)-3-(4-Bromo-phenyl)-2-tert-butoxycarbonylamino-propionic acid methyl ester

: 869569-99-3
tert-butyl (S)-(1-amino-3-(4-bromophenyl)-1-oxopropan-2-yl)carbamate

Guidance literature:: With methanol; ammonia; at -50 - 20 ℃; for 0.25h; Product distribution / selectivity;

Reference yield: 96.0%

: 62129-39-9,79561-82-3
4-bromo-N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-phenylalanine

: 869569-99-3
tert-butyl (S)-(1-amino-3-(4-bromophenyl)-1-oxopropan-2-yl)carbamate

Guidance literature:: 4-bromo-N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-phenylalanine; With 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 0.75h;

With ammonium hydroxide; In N,N-dimethyl-formamide; at 0 ℃; for 72h;

Reference yield:

: 24250-84-8
H-p-BrPhe-OH

: 869569-99-3
tert-butyl (S)-(1-amino-3-(4-bromophenyl)-1-oxopropan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / Reflux

2: sodium hydrogencarbonate / acetone / 20 °C

3: ammonia; methanol / 0.25 h / -50 - 20 °C

With methanol; thionyl chloride; ammonia; sodium hydrogencarbonate; In acetone;