Tert-butyl 2-chloro-4-iodophenylcarbamate

Base Information

Chemical Name:Tert-butyl 2-chloro-4-iodophenylcarbamate
CAS No.:871476-61-8
Molecular Formula:C11H13ClINO2
Molecular Weight:353.587
Hs Code.:
DSSTox Substance ID:DTXSID80700571
Mol file:871476-61-8.mol

Synonyms:TERT-BUTYL 2-CHLORO-4-IODOPHENYLCARBAMATE;871476-61-8;TERT-BUTYL (2-CHLORO-4-IODOPHENYL)CARBAMATE;TERT-BUTYL N-(2-CHLORO-4-IODOPHENYL)CARBAMATE;SCHEMBL9610070;AMY5142;DTXSID80700571;CS-0273182;EN300-3614569;TERT-BUTYL2-CHLORO-4-IODOPHENYLCARBAMATE;TERT-BUTYL(2-CHLORO-4-IODOPHENYL)CARBAMATE

Suppliers and Price of Tert-butyl 2-chloro-4-iodophenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
tert-Butyl(2-chloro-4-iodophenyl)carbamate 97%
5g
$ 752.00

American Custom Chemicals Corporation
TERT-BUTYL-2-CHLORO-4-IODOPHENYLCARBAMATE 95.00%
5MG
$ 499.30

Alichem
tert-Butyl2-chloro-4-iodophenylcarbamate
5g
$ 1111.80

Total 4 raw suppliers

Chemical Property of Tert-butyl 2-chloro-4-iodophenylcarbamate

Chemical Property:

Boiling Point:318.8 °C at 760 mmHg
PKA:12.19±0.70(Predicted)
Flash Point:146.6 °C
PSA：38.33000
Density:1.664 g/cm³
LogP:4.36460
Water Solubility.:at 25 deg C (mg/L): 0.3664
XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:352.96795
Heavy Atom Count:16
Complexity:255

Purity/Quality:

99% ^*data from raw suppliers

tert-Butyl(2-chloro-4-iodophenyl)carbamate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NC1=C(C=C(C=C1)I)Cl

Technology Process of Tert-butyl 2-chloro-4-iodophenylcarbamate

There total 4 articles about Tert-butyl 2-chloro-4-iodophenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 159217-89-7
N-Boc-4-iodoaniline

: 871476-61-8
tert-butyl (2-chloro-4-iodophenyl)carbamate

Guidance literature:: With 1,3-dichloro-5,5-dimethylhydantoin; diisopropylamine hydrochloride; In toluene; at 25 ℃; for 14h; regioselective reaction; Darkness; Green chemistry;
DOI:10.1002/anie.201607388

Reference yield: 84.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 42016-93-3
2-chloro-4-iodoaniline

: 871476-61-8
tert-butyl (2-chloro-4-iodophenyl)carbamate

Guidance literature:: With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃;
DOI:10.1016/j.bmcl.2007.06.012

Reference yield: 79.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 871476-61-8
tert-butyl (2-chloro-4-iodophenyl)carbamate

Guidance literature:: 2-chloro-4-iodoaniline; With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 1.5h;

di-tert-butyl dicarbonate; In tetrahydrofuran;